Robust Metal Additive Manufacturing Process Selection ...

When evaluating and down selecting an AM process, design requirements may greatly reduce options if not dictate the decision. The most common basis for process selection is the complexity and scale of the component. For example, the size of many recent rocket engine designs are based on the limitations of L-PBF machines (Ref 61). Beyond size limits, other criteria may include the required material properties from a process, maturity of the process with certain features or alloys, or even process familiarity. High-level attributes include design requirements (features), process-specific considerations, and microstructural characteristics and properties. While an attempt is made to separately categorize these attributes, they are often integral. The general process selection for aerospace components is shown in Fig. 6 which considers the categories for selection criteria. While some process steps are similar to Fig. 1 there are many detailed aspects that are important to the final process selection not captured in the higher level process steps.

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Process selection attributes for aerospace components. The colors align with process steps in Fig. 2.

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4.1

Overall Design and Process Attributes

Substantial motivation for process selection is derived from the design phase&#;encompassing the material selection, overall part size, feature resolution, complexity, build rates (related to process economics and feature resolution), internal features, and single or multi-alloy builds (Ref 185). There is a continuum of design solutions for AM that include single or multi-part assemblies and the AM process selection may change accordingly. The trade among these aspects are interrelated and iterative (Ref 5). Despite being shown as an iterative trade, the alloy selection itself is generally accepted as the initial input for process selection, narrowing the potential feedstocks and starting the analysis of process availability. Along with the feedstock type, the process parameters are critical to produce successful AM aerospace components and influence the AM process selection. The process parameters govern the design decisions (for successful fabrication) and will impact process capabilities. These impacts are nontrivial and are pertinent for developmental stages where technology demonstration hardware is manufactured. For hardware qualification, the process parameters must be controlled (locked) and shown to be consistent and repeatable, which is tied to the industrial maturity of a given AM process (and consequently the process economics). Clearly there is no single variable to dictate process selection, and the interwoven nature of process attributes&#;ranging from microstructural minutiae to evolving availability&#;warrants detailed discussion.

4.1.1

Overall Part Size

The overall part size is significant aspect for process selection criteria and may prematurely start down selection. A process chosen for build volume alone is not guaranteed to meet the requirements for performance, feature resolution, or material properties for the final part. These considerations should occur in the design phase, where the state of the industry requires continual evaluation.

Commercial machines and custom installations for AM processes provide a nearly linear relation for the build diameter and build height (Ref 24, 61, 114, 193, 261,262,263) as shown in Fig. 7. The maximum build volume for each process is shown in Fig. 7a and aspect ratios for PBF processes from the same are nearly linear. The greatest aspect ratios are typically observed for DED processes and the smallest are for cold spray&#;both of which offer the largest overall build volumes.

Selection of AM processes based on overall build volume. (a) Maximum build diameter and build height for each of the processes. (b) Commercially available and custom AM machines for each of the processes

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The variance in build volume is influenced by build speed, economic factors, waste reduction (even when considering powder recycling). For L-PBF processes, the feedstock material must fill the build box to the highest point printed, well exceeding the total volume of the part. Both solid-state and DED processes deposit material as needed while building and integrated with a robot or gantry system, easily accommodating large build volumes.

The scale of AM machines has significantly grown since . Figure 7b shows various build sizes available worldwide from many of the major aerospace manufacturers and suppliers (with the largest AW-DED size excluded for increased resolution). While there are many options for build volumes, the number of machines available for a given size may be limited in quantity/availability causing significant lead times. While growth of AM build volumes has and continues to increase, PBF machines are limited to parts with the longest dimension being no greater than 1 m (as captured by the gray box in Fig. 7b). The 1 m3 volume for PBF is limited (in availability) commercially where most machines are < 5 00 × 500 mm for PBF. There are many developments at PBF machine manufacturers to increase the overall build volume. While many machines are designed for high mass parts, there may be limitations of mass for turntables (for DED or solid-state processes), build boxes, and other hardware that is not readily available in literature.

4.1.2

Part Complexity, Feature resolution, and Build Rates

Aerospace AM parts can include billets (e.g., forging replacements), near net shape components that require final machining, or high complexity (final, as-built geometry) that only AM processes can produce. Part complexity is directly related to feature resolution and deposition rate. While tendencies are to incorporate high complexity for optimal mass savings or functional performance, aerospace parts are subject to rigorous inspections to determine flight feasibility and with rising complexity comes reduced inspectability. Nondestructive evaluation (NDE) or nondestructive testing (NDT) techniques are limited in their use to adequately inspect parts (Ref 264,265,266) and design complexity also creates challenges in the post-processing stages such as powder removal, -machining, or surface enhancements (polishing) (Ref 267, 268). When selecting a metal AM process, part complexity must be strongly considered (for both internal and external features) as it is related to feature resolution, deposition rate, and inspection capabilities.

Due to inherent process characteristics, each AM process has a minimum size that it can print consistently for specific design features (holes, wall thicknesses, internal channels, lattice structures). In other words, not all AM processes were designed for the highest feature resolution, and some simply cannot provide an acceptable solution for a specified design. For example, the L-PBF process can often build walls, holes, slots, etc. down to 0.2 mm repeatedly, but may result in higher dimensional tolerances (based on Inconel 718) (Ref 269, 270). Adjustments to parameters for L-PBF may allow for features down to 0.1 mm (Ref 271). The LP-DED process cannot build features to that resolution and are typically on the order or 1 mm for wall thicknesses (Ref 272). Other processes such as AW-DED have a minimum feature build size of approximately 2 mm and AFS-D of 10 mm (Ref 131, 192). The ability to repeatedly create high-complexity, ultra-fine features (e.g., internal passages, fine holes, or complex surfaces) by L-PBF and EB-PBF is unrivaled unless interim processing or final machining steps are included. However, PBF processes are competitive with DED processes for the volume of material built per unit of time (build/deposition rate).

Several metal AM systems allow for hybrid manufacturing, incorporating both additive and subtractive manufacturing technologies (Ref 273). Hybrid systems include both the additive portion (using a deposition head or other approach) and a subtractive machining head for interim machining during fabrication. Machining can occur following completion of the deposition process to allow for higher resolution features but may be limited in access. The UAM process requires use of the hybrid subtractive capability to provide the fine feature resolution (Ref 28). Hybrid systems are very common for the LP-DED process and a limited number of systems are available for the LW-DED and AW-DED processes. Integral machining is not feasible for the EBW-DED process due to the vacuum environment. Integrated hybrid machining has been adopted for use in the L-PBF process, but very limited in use (Ref 274, 275).

The feature resolution for each AM process has ranges and is highly dependent on the feedstock, machine hardware configuration and process parameters (Ref 276) as shown in Fig. 8. For example, DED processes such as LP-DED and LW-DED can use different spot sizes, while AW-DED can increase the wire feedstock diameter, and increase deposition rate at a detriment to feature resolution (Ref 277).

Build rate compared to minimum feature size across the AM processes. Data compiled from (Ref 19, 25, 28, 193, 278,279,280,281,282). Approximated data based on current state of the art using existing machines and parameters

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There is clearly a relationship between deposition (build) rate and feature resolution; and the deposition rate is further related to the melt pool size, which varies microstructure (Ref 15). Material properties may be impacted by high heat inputs (used to establish grain growth (Ref 40) to accommodate faster build times. The print speed (material deposited per unit time) is key to shorten manufacturing lead times and is a critical variable for AM process trades yet may have unintended consequences if metallurgical impacts are forgotten.

For forging or casting replacements, the deposition rate is prioritized over feature resolution, assuming all other properties can be met. Fabrication speed one of the greatest advantages of the solid-state processes where no melting occurs. These processes (cold spray, AFS-D, UAM) offer high deposition rates while maintaining a fine grain structure, which is desirable in aerospace parts (Ref 28). A graphical summary of the feature resolution compared to deposition/build rate is shown in Fig. 9. This figure includes many examples of aerospace components for each of the AM processes.

Selection of process based on feature resolution, build/deposition rate and multi-alloys builds. AFS-D image credits to MELDTM Manufacturing, Cold spray image credits to Spee3D, EBW-DED image credits to Sciaky and Lockheed Martin Corporation, AW-DED image credits to Gefertec, LW-DED image credits to Meltio, UAM image credits to Fabrisonic and NASA JPL, LP-DED image shows a Ni-based part manufactured by LMD-p during the DEPOZ project led by IRT Saint-Exupery and Formalloy, L-PBF image credits to Renishaw plc and CellCore GmbH/Sol Solutions Group AG, EB-PBF image credits to Wayland and GE Additive/Arcam. Black text represents melting processes while blue text represents solid-state processes

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4.1.3

Feedstock for AM processes

The designer must consider the supply chain for metal AM (Ref 283), explicitly for the starting feedstock and the AM processing machine. While feedstocks for the most common AM materials are readily available from multiple powder suppliers and can be rapidly deployed, customized, or novel materials may have long lead times for powder production. Wire of many common alloys is readily available for DED processes. Foil and bar are other forms of feedstock, but some are less readily available than powder or wire forms. Additionally, the size of the feedstock (diameter of wire or powder particle size distribution) needed may not always be readily available for a given material. Regardless of composition, form, or novelty, feedstocks may be long-lead time and must be considered when evaluating the entire supply chain.

Powder feedstock requirements depend on the AM process and must be controlled to the chemistry and powder size distribution (PSD) to ensure flowability or spreadability. Many powder alloys are readily available within days according to the PSD required for the AM processes. Even with new materials and custom alloys, the powder supply chain has evolved, and most custom alloyed powder can be obtained in a matter of a few months or less, pending availability of required alloying elements. Many bar, sheet, and wire feedstocks are also commonly available within days. However, custom alloys may require additional processing (e.g., master melt, forging, reducing sheet thickness, or redrawing wire diameter if a specific size is unavailable) and may be more difficult to obtain or with longer lead times. Custom alloys have much longer lead time in these forms due to the multiple processes required: casting, remelts, rolling, and further reduction into forms of barstock or wire (via. drawing and redrawing to size). It is not uncommon for lead times to exceed 20 weeks for custom alloyed wires due to all the required process and pricing can exceed 5x of similar powder forms. Examples of typical feedstocks and sizes are shown in Table 2.

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4.1.4

Single or Multiple Alloy

Some of AM processes allow for multiple alloys (e.g., bimetallic or multi-metallic parts) using different powder, wire, sheet or barstock within the same build operations. Builds with multiple alloys may be readily optimized for mass, thermal, structural, or other design features. Multi-material builds benefit aerospace components through elimination or reduction of joining or post-print assembly operations. Complex designs may make use of multiple materials within a single component without post-processing such as welding or brazing. However, the design requirements may limit the availability of some AM processes or using multiple alloys. The requirements must also consider material compatibility since many of the AM processes involve melting and can form undesirable phases (Ref 284).

Most AM processes allow for multiple alloys, although the metallurgical characterization and full implementation into flight applications is limited to date. As shown in Fig. 9, the DED and solid-state processes allow for multiple materials with additional examples of bimetallic parts shown in Fig. 4. The EB-PBF process does not yet allow for multiple materials, but multiple alloy use in the L-PBF process is being advanced (Ref 166, 285,286,287). Multi-alloys challenges for L-PBF stem from contamination of mixing different powder lots, difficulties in adequately tracking of feedstock lots, and the associated parameter development and control for qualification. Multiple alloys may be incorporated through a secondary operation following initial AM fabrication and machining (if necessary). Then, the secondary AM process adds material of monolithic or multi-alloy composition. An example of this might include flanges deposited with a DED process (higher deposition rate and lower resolution necessary) being added as a secondary operation after final machining of a L-PBF part (high complexity internal features). Some of the AM processes have this capability while others do not. The PBF processes limit features being added later after the build.

4.1.5

Process Economics

While AM offers designers new capabilities to design highly complex components and many sources cite that &#;complexity is free,&#; this complexity also comes at many costs (Ref 288). This may be apparent due to increased build time, build failures, or in necessary post-processing operations. Certain costs are intertwined such as build volume (feedstock usage) with both build time. In turn, multiple costs may be reduced through design optimization (i.e., minimizing part mass while meeting the design intent, design margins, and compensating for distortion/shrinkage (Ref 289). Some reports provided relative cost differences based on the machinery, maintenance, operational cost and feedstock (Ref 19, 290), but detailed direct costs are not easy compared among the processes, since they are based on the part geometry (complexity), feedstock, alloy composition, machine usage and accessibility, post-processing, and the qualification approach required for end-use (Ref 291). Due to subjective factors affecting direct costs, designers must lean on the total cost for each process, which is derived from feedstock cost, setup and programming, machine build time, post-processing operations, as well as supplementary tasks such as engineering and documentation (Ref 292).

Feedstocks in the form of powder, wire, bar, or sheet stock are commonly available for most of the processes, but costs are alloy dependent. Common alloys such as 300 series stainless, Inconel 625 are available off the shelf, although custom alloys or custom sizes can increase costs by 2-5 times since they may require special melts, atomization, or forming operations. An industry survey was conducted to provide a cost comparison for feedstock among the various processes, and results are shown in Fig. 10. There are slight cost differences based on quantity purchased (as expected) and cost variations between individual feedstocks based on the production method. The feedstock supply chain can become more challenging as scarce or custom alloys are developed. This part of the lifecycle must be considered when selecting an appropriate process or alloy itself.

Cost comparison of feedstock for 316L and Inconel 625 ( USD)

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Setup and programming costs for the AM process generally include offline model evaluation, model modifications (support structures), slicing, toolpath or scan strategy development, and any documentation and planning operations. These are considered non-recurring engineering (NRE) costs. Aerospace AM components require stringent documentation and traceability throughout the process, so planning paperwork and travelers may be more extensive. The setup costs may also include build plate machining as well as cleaning and changeover of the machine from one metal alloy to another. The actual build time on the machine is typically based on an hourly rate from start to finish of the part. There are significant differences between the AM processes based on melting and deposition rates including that of L-PBF and EB-PBF (Ref 293). Following the build, post-processing operations will vary based on the process. For most processes, this includes powder removal, support removal, and build plate removal. There are also many post-processing operations such as material characterization and mechanical testing to verify properties of the build. Some references and companies have reported that 70% of the part cost can be derived from pre and post-processing operations (Ref 294).

While there are some economies of scale and learning curves with AM, the unit cost does not significantly vary for increased build quantity (Ref 295,296,297). The NRE costs can be amortized over the production parts, but typically the build time for parts is similar from the first to the hundredth part. While some literature suggest that AM high-volume production is not competitive (Ref 298), it is highly dependent on the part size, material and complexity. In many cases, AM may be the only way to manufacture certain parts (consider the GE fuel nozzles case) and allows for high volume production (Ref 41). There are general trends observed with cost, which can be used to help compare the processes shown in Fig. 11. With AM builds, the primary process cost is based on the overall volume of the material being built (or deposited) as opposed to machined. As overall part volume increases so does cost, but this is highly dependent on the deposition rate. As the deposition rate increases, the cost can decrease. This is where many of the high deposition rate processes such as DED processes, cold spray, and AFS-D has advantages. This deposition rate can come with detrimental impacts to the feature resolution and complexity, which is greatly reduced compared to L-PBF. As the deposition rate increases, the complexity of features decreases, and extra stock must be machined away for critical mating surfaces, holes, flanges, or key features. The additional post-processing step then adds cost. This is a crucial trade of the designer though to evaluate the entire AM process lifecycle including the AM process and post-processing to determine the optimal manufacturing path. The cost trade among AM processes includes the as-built complexity with the post-processing complexity required. The trends shown in Fig. 11 are based on factors including the alloy, process specifics, and part geometry and may not necessarily be linear.

General AM Process cost trends based on part volume and deposition rate. The trends shown are based on factors including the alloy, process specifics, and part geometry and may not necessarily be linear

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An example of cost for an AM liquid rocket engine combustion chamber is shown in Fig. 12. The costs are fully captured due to the reduction in labor hours, material, and multiple processes required with traditional manufacturing. The traditional manufacturing process required a billet of the copper alloy to be produced through forging operations, followed by multiple machining operations of the liner, slotting to form the channels, and finally assembly operations such as plating or brazing to closeout the channels and form the structural jacket (Ref 166, 176). AM processes (i.e., Initial AM Development) allowed for a reduction in cost and schedule to build a chamber using L-PBF GRCop-84 in two-pieces based on machine limitations, followed by EBW-DED cladding of a structural jacket using Inconel 625. As AM processes were more readily available in the supply chain (i.e., Evolving AM Development), the GRCop-42 liner was able to be built in one-piece in a larger PBF machine platform followed be a simplified LP-DED jacket using a commercial vendor.

Cost comparison for a 156 kN (35,000 lbf) Bimetallic Combustion Chamber (based on (Ref 61) in USD)

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4.1.6

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Industrial maturity and Process Availability

Aerospace organizations are infusing metal AM into their system designs (with examples shown in Fig. 13) due to the maturation across metal AM processes and further competition to increase frequency of flights and reduce overall costs (Ref 1, 299, 300). Some of the AM processes are more mature than others due to early industry adoption, standards development for flight applications, and the evolution and characterization of the materials used, which increased the technology readiness levels (TRL) (Ref 301, 302). The most used metal AM process is L-PBF with a significant growth in aerospace applications and machine availability across companies and service vendors. Several flight applications with commercial space and aviation companies demonstrated L-PBF successfully, and L-PBF production was approved for many programs (Ref 1, 303). A TRL of 9 (ongoing flight) has been demonstrated for L-PBF and there is an expansive supply chain available. EB-PBF was demonstrated in flight around and has continued use in aerospace applications, but to a lesser degree than L-PBF (Ref 24). EB-PBF is accessible with various machines across the supply chain but has a limited alloy selection. Public results of LP-DED maturation shows an absolute minimum of TRL 6 (i.e., subsystem model/prototype demonstration in a relevant environment) with component development and demonstration completed in a rocket hot fire environment (Ref 109, 154). There are many suppliers available for production parts using LP-DED, but significantly less than L-PBF.

Examples of select AM components tested on liquid rocket engines to achieve minimum TRL 6. (a) L-PBF GRCop-42 Chamber with LP-DED Inconel 625 nozzle and L-PBF Inconel 625 Injector (Ref 311), (b) Cold spray superalloy jacket and L-PBF copper liner with L-PBF Superalloy Injector. Ariane Group applied the load-bearing structure to the LBM copper chamber with an IMPACT Cold Spray System [Credit: ESA / ArianeGroup GmbH and Impact Innovations], (c) Actively-cooled nozzle with LW-DED closeout jacket with an AW-DED liner (Ref 306), (d) GRCop-84 Chamber with EBW-DED jacket, L-PBF Inconel 718 nozzle film coolant ring, and L-PBF Inconel 625 Injector (Ref 311)

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LW-DED maturity has grown with applications of a regeneratively-cooled nozzle through full-scale systems rocket engine testing, and plans for flight on a future launch vehicle may further maturation (Ref 304,305,306). The LW-DED process availability is limited across the AM supply chain and is a niche process. The AW-DED process has demonstrated a minimum TRL 6 through systems testing (Ref 45, 307). While the AW-DED is extensively researched in academia, the commercial supply chain remains limited in company offerings. EBW-DED was demonstrated for flight applications, but there are limited vendors available that offer the process commercially (Ref 26). Cold spray has been demonstrated in-flight applications and achieved a high TRL; while mostly used for repairs, freeform applications are maturing (Ref 308). Cold spray was demonstrated for freeform and bimetallic applications including hot-fire testing for liquid rocket engine combustion chambers (Ref 166, 309). The number of commercially available cold spray machines for production presently is limited, but the market is growing with new machine manufacturers. AFS-D and UAM are less developed compared to many of the other processes, but research and industrialization is rapidly maturing. The machines for AFS-D and UAM are produced by a single manufacturer each, and commercial availability is extremely limited. UAM has been demonstrated in flight applications reaching TRL 9 (Ref 310).

A growing application implementing AM processes is for maintenance, repair, and overhaul (MRO), which is providing a solution to many obsolescence challenges (Ref 312). Industry adoption of AM processes has led to NASA, European Space Agency (ESA), Federal Aviation Administration (FAA), European Union Aviation Safety Agency (EASA), and standard development organizations (i.e., SAE, ASTM, NIST, AWS) to create qualification and certification specifications and methodologies to allow use of AM processes in flight hardware applications (Ref 8, 313, 314). A main consideration of TRL and industrialization is the maturity of the component development and system testing, database for material properties, design allowables, and classification of material for statistical basis of properties (i.e., A-basis, B-basis). There remains a limited number of alloys and flight hardware that have been qualified and matured for launch systems and aircraft.

4.1.7

Post-Processing

Post-processing is a critical step of the AM lifecycle to ensure that parts meet the final performance requirements. Post-processing can improve the microstructure through various heat treatments to meet the end-use application, ensure that parts meet tolerance for sub-system or system integration, and modify geometric features to meet tolerances or integration. The general post-processing operations that should be evaluated during the design stage include powder removal, support removal, build plate removal, heat treatments, inspections, final machining, cleaning, polishing or surface enhancements, and joining such as welding or brazing (Ref 268). Not all the post-processing operations are required for every part and specific post-processing steps are dependent on the AM process used and program requirements. An example of the various post-processing that may be required for the AM processes is shown in Table 3. From the table, it is observed there are extra steps necessary with the PBF processes that include powder removal and verification along with support removal if they are used. Powder removal and verification is also required for LP-DED, but to a lesser extent since the part is not packed in powder.

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Stress relief is often required for parts prior to removal from the build plate to ensure that residual stresses do not cause distortion (Ref 126, 315, 316). This is only required for the AM processes with higher heat input and not for the solid-state processes. Build plate removal is required for all processes but can be incorporated within the part design or through fixturing for further post-processing operations such as machining. Heat treatments, such as Hot Isostatic Pressing (HIP), homogenization, solution annealing, aging are dependent on the alloy (Ref 41). Certain solid-state processes may not require final heat treatment since the material is deposited below the melting point, but this is dependent on the starting feedstock and properties needed. HIP is often required for cold spray to improve final density since the as-deposited material can result in 1 to 2% porosity (Ref 28, 317). Conformance verification occurs through NDE methods (e.g., structured light scanning (Ref 318), x-ray CT (Ref 319,320,321), neutron CT (Ref 321,322,323,324), acoustic imaging (Ref 325, 326), etc.) as well as search for internal surface/volume defects.

Final machining is often a primary discriminator for post-processing required between the various AM processes. Aerospace components require tightly controlled tolerances and most parts cannot be used in the as-built condition. This is often due to mating surfaces to contain high pressure gases, propellants, fuels, or other fluids. Each of the AM processes produce different surface texture (roughness and waviness) based on the deposition rates and examples are shown in Fig. 14. With the higher deposition rate processes, more stock material is required to accommodate for the waviness of the outside surface. It is apparent that AW-DED has a higher degree of waviness and that more material is necessary to ensure full cleanup for further processing (Ref 89). L-PBF requires far less cleanup since given its higher layer resolution. Other post-processing required are part dependent and may include cleaning, joining (such as welding or brazing for assembly), or surface enhancements to reduce roughness. The AM processes with high texturing and/or roughness (e.g., AW-DED, EBW-DED, Cold spray, AFS-D) require machining.

Comparison of the as-built surface condition and waviness from various metal AM processes. (a) AW-DED nozzle liner, (b) L-PBF pump housing, (c) LW-DED witness sample, (d) LP-DED powerhead shell [Courtesy: NASA]

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Another discriminator between the AM processes is shrinkage and resulting distortion that can impact post-processing, particularly machining, if not properly planned for (Ref 271, 327, 328). The AM processes where material is melted may require additional stock or feature considerations due to shrinkage from the rapid heating and cooling. The solid-state processes discussed here (CS, AFS-D, UAM) do not generally experience shrinkage during the build but may during heat treatments. The surface condition of parts should be considered if used in the as-built (or near final shape) condition. Processes such as L-PBF, EB-PBF and LP-DED may be post-processed with polishing techniques (surface enhancements) to reduce roughness to improve fatigue or flow performance (Ref 31, 329, 330). The varying quality of the surfaces can also impact non-destructive evaluations and applicability of various inspections technologies. Due to the part requirements machining or polishing may also be required to complete the necessary NDE or NDT quality inspections (Ref 264, 266). Proper design for AM will iterate the AM process selection, and should place a strong emphasis on post-processing to meet the design intent (Ref 331).

4.2

Metallurgy and Material Property Considerations

As metal AM processes rapidly mature and are being considered for aerospace component designs and manufacturing, the understanding of materials physics and metallurgy for these different processes must advance. Metallurgy and material properties are a significant attribute that need to be considered when selecting a metal AM process. Material properties are highly dependent on the feedstock and process itself and the post-processing, such as heat treatments. There are several considerations for the metallurgy and resulting material properties. Many of these are interlinked to the other categories for consideration when an alloy is being selected along with the AM process. Some of the considerations for a designer include feedstock, process parameters, component geometry, inhomogeneity, potential process flaws or defects, surface texturing and roughness, thermal stresses, and post-processing heat treatments.

One initial consideration for a design team using AM should include the starting metal feedstock. The end-use part and material are being built or deposited and the end properties are dependent on the starting feedstock composition. Impurities, porosity, and other inconsistencies can impact material outcomes&#;and thermal effects during builds. Specifically, metallurgical changes occur due to varying heat input and cooling rates for the material (Ref 40). Some effects are process specific: the AW-DED process uses a high heat input. The resulting melt pool has more grain growth, resulting in process specific properties (Ref 332). This is characteristic of the DED processes compared to the PBF processes. As cold spray, AFS-D, and UAM processes do not melt the material (only locally plasticizing it), near-wrought properties of the starting feedstock are achievable. Some effects are feature specific&#;material properties are dependent on the local geometry of the component (for AM processes categorized as &#;melting&#; with heat input requirements), where thick and thin sections may be present and there are localized variations in the heating and cooling rates.

When alloys are initially screened for applicability for a specific component, many of the underlying material property information has been collected on more traditionally manufactured specimens. However, when considering the dynamics of the structure-property-processing relationship for materials, a change in the processing of the metal or alloy will have significant impacts on the structure and subsequently the engineered material properties. These AM specific structural variations can be categorized into macrostructural inhomogeneities, microstructural defects, and unique AM microstructural features. By understanding how each AM process can be tuned to influence these variations, engineers can better modify processes to optimize material properties as well as build confidence in new certification approaches to qualify AM parts for aerospace use.

Macrostructural inhomogeneities and flaws can best be viewed as flaws intrinsic to the AM method of choice, generally the off nominal features from the designed build geometry. Within this category there are obvious offenders such as surface topology from the witness marks and the remnants of printing support structures. Less obvious, but equally important are things such as surface texturing (roughness and waviness) or unintentionally filling of engineered void space (e.g., channels, holes, cavities, etc.) with feedstock material. Surface waviness in particular is tied heavily to deposition spot size, so coarser methods such as AFS-D (Ref 333) or AW-DED (Ref 334) can result in more post processing, such as machining. Surface roughness is driven by geometry and features (upskin and downskin), powder size, powder efficiency, process parameters, and melt pool dynamics. These types of flaws have significant impacts on mechanical properties like strength, toughness, and wear resistance as there are now a variety of extrinsic stress risers; these may be overlooked when stresses and strains are initially modeled around designed parts, let alone when parts are manufactured out of geometric tolerances. Methods to mitigate macrostructural surface defects through post-processing are in use and being developed.

Microstructural flaws are equally important when considering their impact on material properties. Most fall into that category of either porosity, lack-of-fusion, or microcracks (Ref 335). Porosity is considered as an inherent defect, occurring due to the intrinsic nature of even a controlled AM process. Pores are always present, but the population of inherent defects is strongly influenced by the AM process execution details (parameters, hardware), the material feedstock, and the amount of process development and control. Powder bed methods are particularly susceptible to porosity, generally due low volumetric energy density that result from un-optimized build parameters (Ref 336,337,338,339). Spherical powder feedstock and tight particle size distribution (PSD) help alleviate these issues, likely influencing adoption as standard practice for powder-based AM.

High thermal stresses, especially those AM methods involving melting of the feedstock, can cause microcracking within printed structures. This is prominent in high melting point alloys where the temperature differential between the build plate and the melt pool are larger, as well as in brittle alloys that cannot withstand significant residual stresses before cracking. Stress buildup is also common in cold spray where high velocity particle impact on the build surface causes plastic deformation, work hardening the material as it is deposited (Ref 87). Preheating build platforms and post-processing heat treatments help alleviate these microstructural defects. However, while heat treatments can frequently alleviate thermal or mechanical residual stresses, severe stresses may still cause deformation and cause out of tolerance conditions of the component (Ref 340). Lessons learned from traditional sintered powder metallurgy as well as the welding field provide valuable insight to the origin and mitigation of microstructural imperfections that can severely impact metal AM processes (Ref 341).

AM of metals can also lead to unique microstructural features not common in traditional subtractive manufacturing methods from feedstocks formed by casting, forging, or rolling. Effectively &#;seeding&#; crystallographic growth of the newly deposited material (on the build plate or previous layers) is not uncommon. This layer-to-layer translation leads to columnar grains across build layers, producing unique grain morphologies shown in Fig. 15 (Ref 342). In conjunction with this grain morphology, preferred crystallographic texture has been observed in metal AM parts, driving the underlying microstructure away from randomly oriented grain isotropy toward anisotropy (Ref 343). Hence, care must be taken in understanding microstructural evolution as a function AM processes, parameters, and heat treatments for the specified alloy since anisotropic materials have properties dependent on build direction (Ref 161, 344,345,346). This can impact the end performance of the properties positively or negatively depending on the desired application (e.g., single crystal turbine blades) (Ref 347).

As-built microstructure of Inconel 625 for the different metal AM processes with build direction (Z) noted by the arrow for all processes. Microstructures from A thru G based on (Ref 317); Image H for AFS-D adopted from (Ref 75). Reprinted from Materials Science and Engineering: A, Vol 694, O.G. Rivera, P.G. Allison, J.B. Jordon, O.L. Rodriguez, L.N. Brewer, Z. McClelland, W.R. Whittington, D. Francis, J. Su, R.L. Martens, N. Hardwick, Microstructures and mechanical behavior of Inconel 625 fabricated by solid-state additive manufacturing, Pages 1-9, Copyright , with permission from Elsevier; Image I courtesy of Fabrisonic. Note: Scales vary to provide the best definition of the as-built microstructure

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Texture evolution is not the same across metal AM build methods either. L-PBF or EB-PBF frequently have Z-directional (build direction) texture due to the insulating nature of the unused powder feedstock in the XY-plane and the dense build structure in the Z-direction. The resulting temperature gradient dictates columnar/textural evolution (Ref 78, 348,349,350,351). However, DED methods such as LP-DED can have X-, Y-, and Z-dependent textural components (Ref 352, 353). UAM has also been shown to produce preferred texture due to extreme plastic deformation, though some are more reminiscent of traditional rolling textures that are also produced through extreme plastic deformation (Ref 354). Other AM methods have the opposite phenomenon, such as cold spray producing planar grains normal to the build direction (Ref 257). AFS-D has such extreme plastic deformation that recrystallization occurs during the printing process identically to traditional FSW microstructures (Ref 75).

Many common aerospace alloys, such as Inconel 625, Stainless 316L, and Ti-6V-4Al are capable of being built using all the AM processes shown in Table 1. Figure 15 shows micrographs of Inconel 625 built using each of the AM processes. The as-built microstructures are observed to various remnants from the build process, while Fig. 16 shows the microstructural evolution of 625 after stress relief, HIP, and solution annealing.

Inconel 625 from AM processes after Stress Relief, HIP, and Solution Annealing per AMS . All images courtesy NASA/UTEP. AFS-D and UAM not shown since comparable heat treatments were not available.

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Both Inconel 625 and Inconel 718 form a delicate balance of metastable phases to produce a wide range of mechanical properties. Figure 17 shows distinct differences in microstructure and mechanical properties of 718, based on AMS heat treatment, that can be attributed to noticeably different grain size and morphology, intrinsic to the different AM processes (Ref 90). In wrought 718, these phases can be tuned by the melting and billet forging processes. By comparison for AM processes, these phases may be carried over from the feedstock (particularly in wire), but phase development is driven primarily by energy input into the feedstock as it melts and by the amount of excess energy absorbed by the material that was previously deposited. In Fig. 18, it is apparent that as laser power (and spot size) increases, both grain size and shape becomes less consistent in Inconel 625 LP-DED. This may be attributed to the physics of the melted area as it cools&#;as laser power increases, local heat increases, and the local freeze time also increases. The larger grain size from the build is also carried through when fully stress relieved, HIP&#;d and solution annealed based on AMS (shown in bottom images of Fig. 18). This phenomenon exacerbates the anisotropic nature of metal AM parts.

Comparison of Inconel 718 tensile properties of select AM processes (L-PBF, LP-DED, AW-DED) compared to wrought using AMS heat treatment. Adapted from (Ref 90).

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Comparison of different spot size and power parameters for Inconel 625 LP-DED shown as-built and after stress relief, HIP, solution annealing (per ASM ). Build direction is denoted with the arrow for all images

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Post-processing improves the physical and metallurgical properties of AM parts. The typical post-processing path is heat treatment to reduce residual stresses from the AM process (also known as a stress relief), followed by a HIP treatment, and concluded with a solutionize and aging process (depending on the alloy and design requirements). A homogenization step can replace the HIP step at similar temperatures and time, although a HIP is preferred to help alleviate any porosity.

The stress relief process is performed below the solution temperature of the material. The residual stresses are reduced through repeated thermal cycling, which causes in local expansion and contraction (Ref 340). Most important to metal AM parts, this step reduces local stress concentrations in corners, small radii, and edges that may have developed during the printing process and may simplify post-processing machining. However, stress relieving can subtly change the dimensioning on built components, bringing them out of tolerance if not properly planned for.

Once stress relieved, it may be necessary to perform a HIP treatment. The HIP process is performed above the solution temperature of the material, aims to reduce porosity (i.e., increase material density, reduce gas permeability), reduce the magnitude of anisotropy, and improve mechanical properties through the reduction of microstructural defects. The HIP process typically results in minor part shrinkage relative to the amount of porosity removed from the part (Ref 355). Following the HIP, further refinement to the microstructure may be necessary through a more traditional solution and aging process depending on the alloy. There is a cumulative change in physical dimensions caused by heat treatments, and designs must include sufficient excess material for post heat treatment cleanup, otherwise the components may not meet geometric requirements.

For some materials such as refractory alloys with high melt temperatures, effective heat treatments for full recrystallization is difficult to achieve and can require specialized facilities outside of conventional treatment furnaces or HIP facilities. Anisotropic microstructures may not be mitigated for these materials, and variability in properties along different build directions is likely (Ref 356,357,358,359,360). The material selection should also include the available supply chain capabilities for post-processing.

The importance of additive manufacturing lies in the many benefits it offers over traditional manufacturing methods. Here are a few reasons why it is important:

Customization: Additive manufacturing allows for the creation of custom parts that would be difficult or impossible to produce with traditional manufacturing methods. This means more customized products can be offered to customers.

Faster time-to-market: Traditional manufacturing processes can take weeks or even months to create a product. With additive manufacturing, a product can be created in a matter of hours or days. This means that companies can get products to market faster and respond more quickly to market-changing demands.

Reduces waste: Traditional manufacturing methods often produce a significant amount of waste material. Additive manufacturing, on the other hand, produces little to no waste because it only uses the exact amount of material needed to create the product.

Reduces costs: Metal additive manufacturing can be more cost-effective than traditional manufacturing methods because it requires fewer materials and can be used to create complex geometries that would be expensive.

Versatility: Parts can be made from a wide range of materials including plastics, metals, ceramics, and composites. This makes it a versatile technology that can be used in a variety of industries, from aerospace and automotive to healthcare and consumer products.

As additive manufacturing technology continues to evolve, it will become increasingly important for companies to incorporate it into their manufacturing processes to remain competitive in the global marketplace.

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